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NEW RESEARCH TOWARDS THE SYNTHESIS OF 1,4-DIBENZYL-1,4,7-TRIAZACYCLONONANE-7-MONOACETATE TO MODEL OXALATE DEGRADING META...

Permanent Link: http://ncf.sobek.ufl.edu/NCFE004889/00001

Material Information

Title: NEW RESEARCH TOWARDS THE SYNTHESIS OF 1,4-DIBENZYL-1,4,7-TRIAZACYCLONONANE-7-MONOACETATE TO MODEL OXALATE DEGRADING METALLOENZYMES
Physical Description: Book
Language: English
Creator: Windsor, Jaclynn
Publisher: New College of Florida
Place of Publication: Sarasota, Fla.
Creation Date: 2013
Publication Date: 2013

Subjects

Subjects / Keywords: Oxalate
Triazacyclononane
Oxalate Oxidase
Genre: bibliography   ( marcgt )
theses   ( marcgt )
government publication (state, provincial, terriorial, dependent)   ( marcgt )
born-digital   ( sobekcm )
Electronic Thesis or Dissertation

Notes

Abstract: Oxalate is a widely abundant compound found in a variety of plants, bacteria, and fungi. Oxalate is a toxic compound and excretion methods are limited in mammals because of the absence of oxalate-degrading enzymes. Accumulation of oxalate can occur via several routes, including genetic defects, dysfunctional fat absorption, excessive dietary consumption, or possibly deficiencies in metabolism of oxalate-precursors like glyoxal. Two manganese-containing metalloenzymes, oxalate oxidase (oxox) and oxalate decarboxylase (oxdc), are able to metabolize this toxic compound via an oxygen-dependent mechanism that is currently undetermined. A functional small molecule mimic of the active sites of oxox and oxdc could provide medicinal benefits to those suffering from hyperoxaluria and other associated conditions, such as calcium oxalate kidney stones. Based on previous work completed in the Sherman lab and with collaborators, the target ligand is 1,4-dibenzyl-1,4,7-triazacyclononane-7-acetate. Although progress has been problematic due to difficulty in removing the protecting tosyl group from the 1,4-dibenzyl-7-tosyl-1,4,7-triazacyclononane, previous students have effectively removed the group while maintaining the integrity of the benzyl groups. The next step in the synthesis, addition of the ethyl acetate arm, was successfully performed in this thesis in a small-scale reaction that was followed by nuclear magnetic resonance spectroscopy. The resulting hydrogen and carbon spectra provide evidence that the ethyl acetate arm was added to the ring. The following work describes the methods used towards the synthesis of the novel ligand.
Statement of Responsibility: by Jaclynn Windsor
Thesis: Thesis (B.A.) -- New College of Florida, 2013
Electronic Access: RESTRICTED TO NCF STUDENTS, STAFF, FACULTY, AND ON-CAMPUS USE
Bibliography: Includes bibliographical references.
Source of Description: This bibliographic record is available under the Creative Commons CC0 public domain dedication. The New College of Florida Libraries, as creator of this bibliographic record, has waived all rights to it worldwide under copyright law, including all related and neighboring rights, to the extent allowed by law.
Local: Faculty Sponsor: Sherman, Suzanne

Record Information

Source Institution: New College of Florida
Holding Location: New College of Florida
Rights Management: Applicable rights reserved.
Classification: local - S.T. 2013 W77
System ID: NCFE004889:00001

Permanent Link: http://ncf.sobek.ufl.edu/NCFE004889/00001

Material Information

Title: NEW RESEARCH TOWARDS THE SYNTHESIS OF 1,4-DIBENZYL-1,4,7-TRIAZACYCLONONANE-7-MONOACETATE TO MODEL OXALATE DEGRADING METALLOENZYMES
Physical Description: Book
Language: English
Creator: Windsor, Jaclynn
Publisher: New College of Florida
Place of Publication: Sarasota, Fla.
Creation Date: 2013
Publication Date: 2013

Subjects

Subjects / Keywords: Oxalate
Triazacyclononane
Oxalate Oxidase
Genre: bibliography   ( marcgt )
theses   ( marcgt )
government publication (state, provincial, terriorial, dependent)   ( marcgt )
born-digital   ( sobekcm )
Electronic Thesis or Dissertation

Notes

Abstract: Oxalate is a widely abundant compound found in a variety of plants, bacteria, and fungi. Oxalate is a toxic compound and excretion methods are limited in mammals because of the absence of oxalate-degrading enzymes. Accumulation of oxalate can occur via several routes, including genetic defects, dysfunctional fat absorption, excessive dietary consumption, or possibly deficiencies in metabolism of oxalate-precursors like glyoxal. Two manganese-containing metalloenzymes, oxalate oxidase (oxox) and oxalate decarboxylase (oxdc), are able to metabolize this toxic compound via an oxygen-dependent mechanism that is currently undetermined. A functional small molecule mimic of the active sites of oxox and oxdc could provide medicinal benefits to those suffering from hyperoxaluria and other associated conditions, such as calcium oxalate kidney stones. Based on previous work completed in the Sherman lab and with collaborators, the target ligand is 1,4-dibenzyl-1,4,7-triazacyclononane-7-acetate. Although progress has been problematic due to difficulty in removing the protecting tosyl group from the 1,4-dibenzyl-7-tosyl-1,4,7-triazacyclononane, previous students have effectively removed the group while maintaining the integrity of the benzyl groups. The next step in the synthesis, addition of the ethyl acetate arm, was successfully performed in this thesis in a small-scale reaction that was followed by nuclear magnetic resonance spectroscopy. The resulting hydrogen and carbon spectra provide evidence that the ethyl acetate arm was added to the ring. The following work describes the methods used towards the synthesis of the novel ligand.
Statement of Responsibility: by Jaclynn Windsor
Thesis: Thesis (B.A.) -- New College of Florida, 2013
Electronic Access: RESTRICTED TO NCF STUDENTS, STAFF, FACULTY, AND ON-CAMPUS USE
Bibliography: Includes bibliographical references.
Source of Description: This bibliographic record is available under the Creative Commons CC0 public domain dedication. The New College of Florida Libraries, as creator of this bibliographic record, has waived all rights to it worldwide under copyright law, including all related and neighboring rights, to the extent allowed by law.
Local: Faculty Sponsor: Sherman, Suzanne

Record Information

Source Institution: New College of Florida
Holding Location: New College of Florida
Rights Management: Applicable rights reserved.
Classification: local - S.T. 2013 W77
System ID: NCFE004889:00001


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